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Ebook Free Nuclear Magnetic Resonance Spectroscopy

Ebook Free Nuclear Magnetic Resonance Spectroscopy

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Nuclear Magnetic Resonance Spectroscopy

Nuclear Magnetic Resonance Spectroscopy


Nuclear Magnetic Resonance Spectroscopy


Ebook Free Nuclear Magnetic Resonance Spectroscopy

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Nuclear Magnetic Resonance Spectroscopy

From the Back Cover

This is the only how-to volume that investigates the spectroscopy of a variety of nuclides other than H and C in depth. It contains extensive reference material and numerous problems, most of which include real spectra. It is written to provide users with the knowledge necessary to choose the most appropriate experiment to obtain the best quality spectra with the ability to fully interpret the data. The book covers basic theory of NMR spectroscopy, spectrum measurement, the chemical shift and examples for selected nuclei, symmetry and NMR spectroscopy, spin-spin coupling and NMR spin systems, typical magnitude of selected coupling constants, nuclear spin relaxation, the nuclear overhauser effect, editing C NMR spectra, two-dimensional NMR spectroscopy, dynamic NMR spectroscopy, lanthanide shift reagents (LSR), NMR of solids. For NMR spectroscopists and analytical chemists.

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Excerpt. © Reprinted by permission. All rights reserved.

It is probably safe to say that NMR spectroscopy is the most broadly utilized spectroscopic technique presently available for obtaining detailed information on chemical systems at the molecular level. Although there are a number of excellent books on NMR spectroscopy, most of the textbooks focus on 1H and 13C NMR spectroscopy and discuss other nuclei only briefly or not at all. Because Fourier Transform (FT) spectrometers are now generally available in both academic and industrial settings, the synthetic chemist can, and often does, routinely investigate the spectroscopy of a variety of nuclides. Moreover, some of the fundamental principles are best illustrated by considering the properties and spectra of nuclei other than 1H and 13C. This book was written as a textbook for senior undergraduate and graduate students who need a reasonably thorough discussion of the subject at an introductory level. It contains a fair amount of chemical-shift and coupling-constant data for seven of the more widely studied nuclides (1H, 11B, 13C, 15N, 19F, 31P, and 195pt) but is not a compendium of such data. References to compendia are given in the appropriate places in the text. The book is largely empirical, but the theoretical basis for most of the more important aspects is presented. I have attempted to explain each of the various experiments at a level such that the reader can ascertain which among several alternatives would be the best experiment to use. The practitioner should always ask, "What information do I want to obtain?" Then the best, and hopefully easiest, experiments can be chosen to provide that information most expeditiously. Since students often learn this type of material best by solving problems, a large number of practice problems have been included. The majority of them involve actual spectra. The problems have been chosen to represent the concepts discussed in the book, but, of course, are biased by my own interests. An answer book containing detailed solutions is available. Some figures have been taken from the literature, and acknowledgments are given in the appropriate captions. I wish to thank Dr. George A. Gray of Varian Associates, Mr. Lewis W. Cary and Dr. Stephan E. Boiadjiev of the University of Nevada, and Professor Roderick E. Wasylishen of Dalhousie University for several of the spectra reproduced herein. I am also grateful to the many students at UNR who have endured the various forms of this book in my classes. I appreciate their comments, their insightful and probing questions, and their encouragement to complete the book.

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Product details

Paperback: 464 pages

Publisher: Prentice Hall; 1 edition (July 18, 2002)

Language: English

ISBN-10: 0130334510

ISBN-13: 978-0130334510

Product Dimensions:

8 x 1.1 x 10 inches

Shipping Weight: 2.4 pounds (View shipping rates and policies)

Average Customer Review:

2.4 out of 5 stars

2 customer reviews

Amazon Best Sellers Rank:

#3,743,077 in Books (See Top 100 in Books)

Oh my God. This book, in one word, sucks. It's horrible. The book is very computational based, filled to the brim with theoretical equations.I could go on about how it sucks, but essentially, chapter 1 is the only good part about this book. Chapter 1 is the most helpful of them all and is a summary of the first (about) 5 chapters.

This book is decent if you are new to the field of NMR or need a quick refresher. Though there are better introductory texts on NMR, this book explains the basic concepts of spin, chemical shielding, chemical shifts, etc well enough for an undergrad to be able to follow along. It does cover the basic pulse sequences and experiments you would expect to run in any organic chemistry lab. This book is lacking in two main areas. First, it is a terribly dry book to read as it explanations only scratch the surface of the science. Second, its discussion of multi-dimensional NMR is extraordinarily basic. It does have a few discussions on basic experiments such as HMQC, HETCOR and COSY. If you are above the novice level in NMR I would suggest skipping this book and going with something like Jacobsen, which has a much better overall discussion of the field and covers topics ranging from simple 1D experiments to protein NMR. With all of this being said, it is a fairly cheap book which will allow you to begin to understand the field.

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